C₂₉H₄₅N₇O₇

Base Information

Chemical Name:C₂₉H₄₅N₇O₇
CAS No.:1372814-26-0
Molecular Formula:C₂₉H₄₅N₇O₇
Molecular Weight:603.719
Hs Code.:

C<sub>29</sub>H<sub>45</sub>N<sub>7</sub>O<sub>7</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₅N₇O₇

Chemical Property:

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Technology Process of C₂₉H₄₅N₇O₇

There total 6 articles about C₂₉H₄₅N₇O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372814-16-8
H-L-Phe-Aib₄-GlyNH₂

: 75-36-5
acetyl chloride

: 1372814-26-0
C₂₉H₄₅N₇O₇

Guidance literature:: With pyridine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/anie.201107583

Reference yield:

: 1187839-36-6
C₁₆H₂₆N₆O₄

: 1372814-26-0
C₂₉H₄₅N₇O₇

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / acetonitrile / 72 h / Reflux; Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / Inert atmosphere

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 20 °C / Inert atmosphere

5: pyridine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C

With pyridine; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.201107583

Reference yield:

: 1187839-35-5
N₃Aib₄-OH

: 1372814-26-0
C₂₉H₄₅N₇O₇

Guidance literature:: Multi-step reaction with 6 steps

1: 3 h / 120 °C / Inert atmosphere

2: triethylamine / acetonitrile / 72 h / Reflux; Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / Inert atmosphere

4: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 0 - 20 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen; acetic acid / ethanol / 20 °C / Inert atmosphere

6: pyridine / dichloromethane; N,N-dimethyl-formamide / 0 - 20 °C

With pyridine; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/anie.201107583