3-phenylpsoralen

Base Information

Chemical Name:3-phenylpsoralen
CAS No.:78045-67-7
Molecular Formula:C₁₇H₁₀O₃
Molecular Weight:262.265
Hs Code.:

Synonyms:

Suppliers and Price of 3-phenylpsoralen

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenylpsoralen

Chemical Property:

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Technology Process of 3-phenylpsoralen

There total 4 articles about 3-phenylpsoralen which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6468-96-8
7-Hydroxy-3-phenyl-chromen-2-one

: 78045-67-7
3-phenylpsoralen

Guidance literature:: Multi-step reaction with 4 steps

1: 2.2 g / iodine, periodic acid / ethanol / 2 h / Ambient temperature

2: 0.8 g / K₂CO₃ / acetone / 6 h / Heating

3: 0.2 g / N,N-dimethylaniline / 6 h / Heating

4: 1) osmium tetraoxide, potassium periodate , 2) PPA / 1) ethyl acetate, water

With osmium(VIII) oxide; potassium metaperiodate; iodine; potassium carbonate; N,N-dimethyl-aniline; periodic acid; In ethanol; acetone;

Reference yield:

: 77712-81-3
7-hydroxy-8-iodo-3-phenyl-2H-1-benzopyran-2-one

: 78045-67-7
3-phenylpsoralen

Guidance literature:: Multi-step reaction with 3 steps

1: 0.8 g / K₂CO₃ / acetone / 6 h / Heating

2: 0.2 g / N,N-dimethylaniline / 6 h / Heating

3: 1) osmium tetraoxide, potassium periodate , 2) PPA / 1) ethyl acetate, water

With osmium(VIII) oxide; potassium metaperiodate; potassium carbonate; N,N-dimethyl-aniline; In acetone;