(1R,2R,3R*)-1,2-diphenyl-1,3-dimethoxybutane

Base Information

Chemical Name:(1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane
CAS No.:143120-72-3
Molecular Formula:C₁₈H₂₂O₂
Molecular Weight:270.371
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane

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Technology Process of (1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane

There total 4 articles about (1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4110-75-2
(E)-(2-methoxyvinyl)benzene

: 143064-66-8,143120-72-3
(1R*,2R*,3S*)-1,2-diphenyl-1,3-dimethoxybutane

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / 4-MeC₆H₄SO₃H*H₂O / 1) 60 deg C, 20 min; 2) room temperature, 1 week

2: toluene / Heating

With toluene-4-sulfonic acid; In toluene;
DOI:10.1021/jo00044a030

Reference yield:

: 4110-75-2
(E)-(2-methoxyvinyl)benzene

: 143064-66-8,143120-72-3
(1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane

Guidance literature:: Multi-step reaction with 2 steps

1: 43 percent / 4-MeC₆H₄SO₃H*H₂O / 1) 60 deg C, 20 min; 2) room temperature, 1 week

2: toluene / Heating

With toluene-4-sulfonic acid; In toluene;
DOI:10.1021/jo00044a030

Reference yield:

: 3-methoxy-2,3-diphenyl-1-trimethylsilyl-1-propanone

: 143064-66-8,143120-72-3
(1R*,2R*,3R*)-1,2-diphenyl-1,3-dimethoxybutane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / tetrahydrofuran; hexane / -78 °C

2: 94 percent / TBAF / dimethylformamide / 24 h / heating

3: 87 percent / NaH / tetrahydrofuran / 6 h / Heating

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2003.08.050