2',4'-Dimethoxyphenoxyacetonitrile

Base Information

Chemical Name:2',4'-Dimethoxyphenoxyacetonitrile
CAS No.:149312-73-2
Molecular Formula:C₁₀H₁₁NO₃
Molecular Weight:193.202
Hs Code.:

Synonyms:

Suppliers and Price of 2',4'-Dimethoxyphenoxyacetonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2',4'-Dimethoxyphenoxyacetonitrile

Chemical Property:

Purity/Quality:

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Technology Process of 2',4'-Dimethoxyphenoxyacetonitrile

There total 2 articles about 2',4'-Dimethoxyphenoxyacetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 13330-65-9
2,4-dimethoxyphenol

: 107-14-2
chloroacetonitrile

: 149312-73-2
2',4'-Dimethoxyphenoxyacetonitrile

Guidance literature:: With 8-crown-6 ether; potassium carbonate; In acetone; for 1h; Heating;

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 149312-73-2
2',4'-Dimethoxyphenoxyacetonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 30 percent H₂O₂, SeO₂, 2) aq. NaOH / 1) CH₂Cl₂, r.t., 12 h

2: 80 percent / 8-crown-6-ether, K₂CO₃ / acetone / 1 h / Heating

With sodium hydroxide; selenium(IV) oxide; 8-crown-6 ether; dihydrogen peroxide; potassium carbonate; In acetone;

Reference yield:

: 149312-73-2
2',4'-Dimethoxyphenoxyacetonitrile

: Glyasperin E dimethyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: 1) gaseous HCl, ZnCl₂, 2) H₂O / 1) THF, a) ice bath, 4 h, b) to r.t., overnight, 2) reflux, 30 min

2: 75 percent / pyridine / 72 h / Ambient temperature

3: 91 percent / H₂O, K₂CO₃ / acetone / 0.5 h / 60 °C

4: 38 percent / 0.17 h / 220 - 240 °C

5: 96 percent / K₂CO₃ / acetone / 0.5 h / Heating

6: 3 percent / KOH / methanol / 0.5 h / Ambient temperature

With pyridine; hydrogenchloride; potassium hydroxide; water; potassium carbonate; zinc(II) chloride; In methanol; acetone;