3--1,2,4-trimethylquinolinium

Base Information

• Chemical Name: 3--1,2,4-trimethylquinolinium
• CAS No.: 104785-61-7
• Molecular Formula: C₂₂H₂₅N₂O
• Molecular Weight: 333.453
• Mol file: 104785-61-7.mol

Synonyms:

Chemical Property of 3--1,2,4-trimethylquinolinium

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3--1,2,4-trimethylquinolinium

There total 4 articles about 3--1,2,4-trimethylquinolinium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3--1,2,4-trimethyl-1,4-dihydroquinoline (104465-70-5,104465-71-6,118609-08-8,134623-72-6,134623-73-7) → 3--1,2,4-trimethylquinolinium (104785-61-7,118609-07-7,128706-97-8,128779-23-7,149818-14-4) + 3--1,2,4-trimethylquinolinium (104785-61-7,118609-07-7,128706-97-8,128779-23-7,149818-14-4)

Guidance literature:

With copper(II) bis(dibenzoylmethanate); magnesium perchloride; In tetrahydrofuran; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature; dark; further cation and ligands;

DOI:10.1016/0040-4039(88)85090-1

Reference yield:

3--1,2,4-trimethyl-1,4-dihydroquinoline (104465-70-5,104465-71-6,118609-08-8,134623-72-6,134623-73-7) → 3--1,2,4-trimethylquinolinium (104785-61-7,118609-07-7,128706-97-8,128779-23-7,149818-14-4) + 3--1,2,4-trimethylquinolinium (104785-61-7,118609-07-7,128706-97-8,128779-23-7,149818-14-4)

Guidance literature:

With copper(II) bis(dibenzoylmethanate); magnesium perchloride; In tetrahydrofuran; for 24h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature; dark; further cation and ligands;

DOI:10.1016/0040-4039(88)85090-1

Reference yield:

(4R)-3--1,2,4-trimethyl-1,4-dihydroquinoline (104465-70-5) → 3-(N-Methyl-N-α-methylbenzylcarbamoyl)-1,2,4-trimethylquinolinium (104785-61-7)

Guidance literature:

With 2,5-Dichloro-1,4-benzoquinone; In acetonitrile; for 24h; Product distribution; Mechanism; Ambient temperature; other reagents, also in the presence of magnesium perchlorate, other quinoline, also with pyridine derivatives;

DOI:10.1246/bcsj.64.81

upstream raw materials:

(4R)-3--1,2,4-trimethyl-1,4-dihydroquinoline

4S,11R-3-(N-methyl-N-α-methylbenzyl)carbamoyl-1,2,4-trimethyl-1,4-dihydroquinoline

3--1,2,4-trimethyl-1,4-dihydroquinoline