C₅₆H₇₅N₅O₁₈

Base Information

Chemical Name:C₅₆H₇₅N₅O₁₈
CAS No.:161909-28-0
Molecular Formula:C₅₆H₇₅N₅O₁₈
Molecular Weight:1106.23
Hs Code.:

C<sub>56</sub>H<sub>75</sub>N<sub>5</sub>O<sub>18</sub>

Synonyms:

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Chemical Property of C₅₆H₇₅N₅O₁₈

Chemical Property:

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Technology Process of C₅₆H₇₅N₅O₁₈

There total 4 articles about C₅₆H₇₅N₅O₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 161909-28-0
C₅₆H₇₅N₅O₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / dimethylformamide / 4 h / Ambient temperature

2: 72 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 40 °C / 20 Torr

3: 1.) pyridinium trifluoroacetate, DMSO, dicyclohexylcarbodiimide, 2.) oxalic acid dihydrate / 1.) C₆H₆, r.t., overnight, 2.) C₆H₆, dioxane, r.t., 30 min

With pyridine; pyridinium trifluroacetate; oxalic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.47.821

Reference yield:

: 3,2',6'-tris(N-tert-butoxycarbonyl)dibekacin

: 161909-28-0
C₅₆H₇₅N₅O₁₈

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / dimethylformamide / 4 h / Ambient temperature

2: 72 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 40 °C / 20 Torr

3: 1.) pyridinium trifluoroacetate, DMSO, dicyclohexylcarbodiimide, 2.) oxalic acid dihydrate / 1.) C₆H₆, r.t., overnight, 2.) C₆H₆, dioxane, r.t., 30 min

With pyridine; pyridinium trifluroacetate; oxalic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.47.821

Reference yield:

: 161909-27-9
1,3''-bis(N-benzyloxycarbonyl)-3,2',6'-tris(N-tert-butoxycarbonyl)dibekacin

: 161909-28-0
C₅₆H₇₅N₅O₁₈

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / p-toluenesulfonic acid / dimethylformamide / 1 h / 40 °C / 20 Torr

2: 1.) pyridinium trifluoroacetate, DMSO, dicyclohexylcarbodiimide, 2.) oxalic acid dihydrate / 1.) C₆H₆, r.t., overnight, 2.) C₆H₆, dioxane, r.t., 30 min

With pyridinium trifluroacetate; oxalic acid; toluene-4-sulfonic acid; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide;
DOI:10.7164/antibiotics.47.821