C₂₈H₃₇NO₆Si

Base Information

Chemical Name:C₂₈H₃₇NO₆Si
CAS No.:154968-03-3
Molecular Formula:C₂₈H₃₇NO₆Si
Molecular Weight:511.69
Hs Code.:

C<sub>28</sub>H<sub>37</sub>NO<sub>6</sub>Si

Synonyms:

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Chemical Property of C₂₈H₃₇NO₆Si

Chemical Property:

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Technology Process of C₂₈H₃₇NO₆Si

There total 11 articles about C₂₈H₃₇NO₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 130539-12-7
N-Benzyloxycarbonyl-1,5-dideoxy-1,5-imino-D-glucitol

: 154968-03-3
C₂₈H₃₇NO₆Si

Guidance literature:: Multi-step reaction with 10 steps

1: 65 percent / TosOH

2: 68 percent / Bu₂SnO, NEt₃ / 24 h / 25 °C

3: Hunig's base

4: Bu₄NOH / dioxane; H₂O / 25 °C

5: DMSO / trifluoroacetic acid / 3 h / -70 - -30 °C

6: 43 percent

7: 85 percent / Bu₄NF / 18 h / 25 °C

8: 65 percent / Bu₄NF / Heating

9: 95 percent

10: m-CPBA / CH₂Cl₂

With tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydroxide; di(n-butyl)tin oxide; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; water; trifluoroacetic acid;
DOI:10.1016/0040-4039(96)00021-4

Reference yield:

: 19130-96-2
1,5-dideoxy-1,5-imino-D-glucitol

: 154968-03-3
C₂₈H₃₇NO₆Si

Guidance literature:: Multi-step reaction with 11 steps

1: 60 percent / Na₂CO₃ / H₂O

2: 65 percent / TosOH

3: 68 percent / Bu₂SnO, NEt₃ / 24 h / 25 °C

4: Hunig's base

5: Bu₄NOH / dioxane; H₂O / 25 °C

6: DMSO / trifluoroacetic acid / 3 h / -70 - -30 °C

7: 43 percent

8: 85 percent / Bu₄NF / 18 h / 25 °C

9: 65 percent / Bu₄NF / Heating

10: 95 percent

11: m-CPBA / CH₂Cl₂

With tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydroxide; di(n-butyl)tin oxide; sodium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; water; trifluoroacetic acid;
DOI:10.1016/0040-4039(96)00021-4

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 154968-03-3
C₂₈H₃₇NO₆Si

Guidance literature:: Multi-step reaction with 11 steps

1: 60 percent / Na₂CO₃ / H₂O

2: 65 percent / TosOH

3: 68 percent / Bu₂SnO, NEt₃ / 24 h / 25 °C

4: Hunig's base

5: Bu₄NOH / dioxane; H₂O / 25 °C

6: DMSO / trifluoroacetic acid / 3 h / -70 - -30 °C

7: 43 percent

8: 85 percent / Bu₄NF / 18 h / 25 °C

9: 65 percent / Bu₄NF / Heating

10: 95 percent

11: m-CPBA / CH₂Cl₂

With tetrabutyl ammonium fluoride; tetra(n-butyl)ammonium hydroxide; di(n-butyl)tin oxide; sodium carbonate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In 1,4-dioxane; dichloromethane; water; trifluoroacetic acid;
DOI:10.1016/0040-4039(96)00021-4