O-dibenzyl-β-conidendrine

Base Information

Chemical Name:O-dibenzyl-β-conidendrine
CAS No.:89067-60-7
Molecular Formula:C₃₄H₃₂O₆
Molecular Weight:536.624
Hs Code.:

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Suppliers and Price of O-dibenzyl-β-conidendrine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-dibenzyl-β-conidendrine

Chemical Property:

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Technology Process of O-dibenzyl-β-conidendrine

There total 17 articles about O-dibenzyl-β-conidendrine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 89067-59-4,89104-62-1
O-dibenzylhydroxymatairesinol

: 89067-60-7,105817-19-4
(d,l)-O-dibenzyl α-conidendrine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 10 ℃; for 3h;
DOI:10.1016/S0040-4020(01)87617-1

Reference yield: 86.0%

: 89067-60-7,105817-19-4
(d,l)-O-dibenzyl α-conidendrine

: 89067-60-7,105817-19-4
O-dibenzyl-β-conidendrine

Guidance literature:: With sodium methylate; In methanol; dichloromethane; for 1h; Heating;
DOI:10.1016/S0040-4020(01)87617-1

Reference yield:

: 72724-00-6
1-(benzyloxy)-4-(bromomethyl)-2-methoxybenzene

: 89067-60-7,105817-19-4
(d,l)-O-dibenzyl α-conidendrine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) lithium diisopropylamide; 2.) HMPT / 1.) tetrahydrofurane, -80 deg C; 2.) THF, -80 deg C, 1 h 30 min

2: 86 percent / BF₃-Et₂O, HgO / tetrahydrofuran; H₂O / Ambient temperature

3: 76.5 percent / sodium borohydride / methanol / 3 h / 0 °C

4: 95 percent / CF₃COOH / CH₂Cl₂ / Ambient temperature

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; boron trifluoride diethyl etherate; trifluoroacetic acid; mercury(II) oxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1246/cl.1983.1543