acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo

Base Information

Chemical Name:acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo
CAS No.:59259-40-4
Molecular Formula:C₁₄H₁₃ClO₂
Molecular Weight:248.709
Hs Code.:

Synonyms:

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Chemical Property of acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo

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Technology Process of acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo

There total 15 articles about acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28446-72-2
4-chlorocinnamonitrile

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3endo-(4-chloro-phenyl)-norborn-5-ene-2exo-carboxylic acid

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3exo-(4-chloro-phenyl)-norborn-5-ene-2endo-carboxylic acid

: (1S,2R,3S,4R)-3-(4-Chloro-phenyl)-bicyclo[2.2.1]hept-5-ene-2-carbonitrile

Guidance literature:: With hydroquinone; In benzene; at 180 ℃; for 144h;
DOI:10.1021/jm980566m

Reference yield:

: 28446-72-2
4-chlorocinnamonitrile

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3endo-(4-chloro-phenyl)-norborn-5-ene-2exo-carboxylic acid

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
(+/-)-3exo-(4-chloro-phenyl)-norborn-5-ene-2endo-carboxylic acid

: (1S,2R,3S,4R)-3-(4-Chloro-phenyl)-bicyclo[2.2.1]hept-5-ene-2-carbonitrile

Guidance literature:: With hydroquinone; In benzene; at 180 ℃; for 144h;
DOI:10.1021/jm980566m

Reference yield:

: 1615-02-7,940-62-5
3-(4-chlorophenyl)prop-2-enoic acid

: 59259-40-4,59286-06-5,59286-10-1,81570-33-4
acide p-chloro phenyl-3 exo bicyclo<2.2.1> heptene-5 carboxylique-2 exo

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / dioxane / 24 h / Irradiation

2: 2.) I₂, KI, aq. Na₂CO₃ / 1.) 140 deg C, 4 d

With iodine; sodium carbonate; potassium iodide; In 1,4-dioxane;
DOI:10.1021/jm980566m