(C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅

Base Information

Chemical Name:(C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅
CAS No.:136052-32-9
Molecular Formula:C₂₆H₄₅NO₂Sn
Molecular Weight:522.359
Hs Code.:

(C<sub>4</sub>H<sub>9</sub>)3SnC<sub>6</sub>H<sub>9</sub>(CH<sub>3</sub>)OCONHC<sub>6</sub>H<sub>5</sub>

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Chemical Property of (C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅

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Technology Process of (C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅

There total 1 articles about (C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 126300-46-7
2-methyl-1-tributylstannyl cyclohexanol

: 103-71-9
phenyl isocyanate

: 136052-32-9
(C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅

Guidance literature:: In pentane; byproducts: 1,3-diphenylurea; react. under an inert atmosphere; addn. of phenyl isocyanate soln. to Sn-compound in soln. at room temp. (molar ratio 2:1), stirred at reflux for 5h, pptn.; ppt. removed by filtration, cooled to -20°C overnight, pptn. of last traces of diphenylurea, solvent and unreacted isocyanate removed under reduced pressure;

Reference yield: 43.0%

: 136052-32-9
(C₄H₉)3SnC₆H₉(CH₃)OCONHC₆H₅

: 100073-21-0
(C₄H₉)3SnC₆H₈(CH₃)

Guidance literature:: In gas; byproducts: hexabutylditin; placing starting material in a porcelain cup in the sublimation chamber of a flash vac. thermolysis apparatus, react. at 800-850°C in the main oven and 250-300°C in the sublimation oven (10E-2 mm), oven packed with broken porcelain; vapors quenched on a dewar cold finger, pyrolysis tube cooled to room temp., product washed with ether from the dewar surface, ether evapd., chromy. (florisil);