methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Base Information

Chemical Name:methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate
CAS No.:109639-02-3
Molecular Formula:C₂₂H₃₅N₂O₇P
Molecular Weight:470.503
Hs Code.:

methyl N-<<methoxy<1-<N-<(phenylmethoxy)carbonyl>amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Chemical Property:

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Technology Process of methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

There total 6 articles about methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (S)-4-Methyl-2-trichloromethoxycarbonylamino-pentanoic acid methyl ester

: C₁₇H₃₀NO₄PSi

: 109639-02-3,109716-95-2,109716-96-3,109716-97-4
methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1.5h; Yield given;
DOI:10.1021/jm00392a014

Reference yield:

: 2666-93-5
(S)-Leu-OMe

: 109639-02-3,109716-95-2,109716-96-3,109716-97-4
methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.5 h / 22 °C

2: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

With triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00392a014

Reference yield:

: 109638-99-5
(+/-)-1-benzyloxycarbonylamino-3-methylbutylphosphonous acid

: 109639-02-3,109716-95-2,109716-96-3,109716-97-4
methyl N-<amino>-3-methylbutyl>phosphinyl>carbonyl>-L-leucinate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / methanol; diethyl ether / 0.5 h / 22 °C

2: Et₃N / CH₂Cl₂ / 0.5 h

3: Et₃N / CH₂Cl₂ / 1.5 h / 0 °C

With triethylamine; In methanol; diethyl ether; dichloromethane;
DOI:10.1021/jm00392a014