2-[Hydrazinylidene(phenyl)methyl]pyridine

Base Information

• Chemical Name: 2-[Hydrazinylidene(phenyl)methyl]pyridine
• CAS No.: 56009-91-7
• Molecular Formula: C12H11 N3
• Molecular Weight: 197.2358
• DSSTox Substance ID: DTXSID90971396

Synonyms:56009-91-7;SCHEMBL9768821;phenyl-2-pyridylketone hydrazone;DTXSID90971396;Phenyl 2-pyridyl ketone hydrazone;2-[hydrazinylidene(phenyl)methyl]pyridine

Chemical Property of 2-[Hydrazinylidene(phenyl)methyl]pyridine

Chemical Property:

• Vapor Pressure: 3.94E-05mmHg at 25°C
• Boiling Point: 352.1°C at 760 mmHg
• Flash Point: 166.7°C
• Density: 1.12g/cm³
• XLogP3: 1.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 197.095297364
• Heavy Atom Count: 15
• Complexity: 219

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NN)C2=CC=CC=N2

Technology Process of 2-[Hydrazinylidene(phenyl)methyl]pyridine

There total 2 articles about 2-[Hydrazinylidene(phenyl)methyl]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

phenyl(pyridin-2-yl)methanone (91-02-1) → 2-(hydrazono(phenyl)methyl)pyridine (56009-91-7)

Guidance literature:

With hydrazine hydrate; In ethanol; for 2h; Reflux;

DOI:10.1039/c8nj01212a

Reference yield:

→ 2-(hydrazono(phenyl)methyl)pyridine (56009-91-7)

Guidance literature:

(6a), Hydrazin;

DOI:10.1021/ja00859a014

Reference yield: 91.0%

2-(hydrazono(phenyl)methyl)pyridine (56009-91-7) → 3-phenyl-[1,2,3]triazolo[1,5-a]pyridine (832-81-5)

Guidance literature:

With [bis(acetoxy)iodo]benzene; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1080/00397910008087337

upstream raw materials:

phenyl(pyridin-2-yl)methanone

Downstream raw materials:

3-phenyl-[1,2,3]triazolo[1,5-a]pyridine

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