PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄

Base Information

• Chemical Name: PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄
• CAS No.: 590419-01-5
• Molecular Formula: BF₄*C₃₃H₄₃NOPPd
• Molecular Weight: 693.909

Synonyms:

Chemical Property of PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄

Chemical Property:

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Technology Process of PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄

There total 4 articles about PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdCOP(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

PdNCCH3P(C6H2(CH3)3)2CH2NC5H2(C4H9)CCH2(CH3)2(1+)*BF4(1-)=PdNCCH3P(C6H2(CH3)3)2CH2NC5H2C8H17BF4 (590418-97-6) + carbon monoxide (201230-82-2) → PdCOP(C6H2(CH3)3)2CH2NC5H2(C4H9)CCH2(CH3)2(1+)*BF4(1-)=PdCOP(C6H2(CH3)3)2CH2NC5H2C8H17BF4 (590419-01-5)

Guidance literature:

In dichloromethane; a soln. of complex in CH2Cl2 was bubbled with CO at ambient temp. for 10min; filtered, concd., diethyl ether was added, ppt. was filtered off, washedwith diethyl ether; elem. anal.;

DOI:10.1039/b212169g

Reference yield:

(PdClCH3P(C6H2(CH3)3)2CH2NC5H2(C4H9)2)2 (590418-92-1) → PdCOP(C6H2(CH3)3)2CH2NC5H2(C4H9)CCH2(CH3)2(1+)*BF4(1-)=PdCOP(C6H2(CH3)3)2CH2NC5H2C8H17BF4 (590419-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane

2: dichloromethane

In dichloromethane;

DOI:10.1039/b212169g

Reference yield:

2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine (590418-90-9) → PdCOP(C6H2(CH3)3)2CH2NC5H2(C4H9)CCH2(CH3)2(1+)*BF4(1-)=PdCOP(C6H2(CH3)3)2CH2NC5H2C8H17BF4 (590419-01-5)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane

2: dichloromethane

3: dichloromethane

In dichloromethane;

DOI:10.1039/b212169g

upstream raw materials:

PdNCCH₃P(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)CCH₂(CH₃)2⁽¹⁺⁾*BF₄^(1-)=PdNCCH₃P(C₆H₂(CH₃)3)2CH₂NC₅H₂C₈H₁₇BF₄

carbon monoxide

2-{[bis-(2,4,6-trimethyl-phenyl)-phosphanyl]-methyl}-4,6-di-tert-butyl-pyridine

(PdClCH₃P(C₆H₂(CH₃)3)2CH₂NC₅H₂(C₄H₉)2)2

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