Technology Process of C68H100N4O2S
There total 8 articles about C68H100N4O2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide; triphenylphosphine / dichloromethane / Inert atmosphere
2.1: lithium / diethyl ether / Inert atmosphere
2.2: Inert atmosphere
3.1: acetic acid / Inert atmosphere
4.1: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); N-Bromosuccinimide; triphenyl-arsane; lithium; N-ethyl-N,N-diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; diethyl ether; dichloromethane; acetic acid;
DOI:10.1021/jp2000738
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: lithium / diethyl ether / Inert atmosphere
1.2: Inert atmosphere
2.1: acetic acid / Inert atmosphere
3.1: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; lithium; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; diethyl ether; acetic acid;
DOI:10.1021/jp2000738
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / N,N-dimethyl-formamide / Inert atmosphere
2: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triphenylphosphine / Inert atmosphere
3: sodium hydroxide / tetrahydrofuran; methanol / Inert atmosphere
4: tris-(dibenzylideneacetone)dipalladium(0); triphenyl-arsane; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere
With
piperidine; bis-triphenylphosphine-palladium(II) chloride; tris-(dibenzylideneacetone)dipalladium(0); copper(l) iodide; triphenyl-arsane; potassium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium hydroxide;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1021/jp2000738