Technology Process of C60H87N7O11
There total 14 articles about C60H87N7O11 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
methanol;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 9 steps
1: methanol; N-ethyl-N,N-diisopropylamine / 20 °C / Inert atmosphere
2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C
3: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
4: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
5: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
6: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
7: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
8: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C
9: N-ethyl-N,N-diisopropylamine / methanol / 20 °C / Inert atmosphere
With
methanol; palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/ja109665t
- Guidance literature:
-
Multi-step reaction with 8 steps
1: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C
2: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
3: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
4: dicyclohexyl-carbodiimide / tetrahydrofuran / 3 h / 20 °C
5: sodium hydrogencarbonate / tetrahydrofuran; water / 48 h / 20 °C
6: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 760.05 Torr
7: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 48 h / 20 °C
8: N-ethyl-N,N-diisopropylamine / methanol / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; water; hydrogen; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; lithium hydroxide;
In
tetrahydrofuran; methanol; water;
DOI:10.1021/ja109665t