(CF₃)GeH₂(CH₃)

Base Information

• Chemical Name: (CF₃)GeH₂(CH₃)
• CAS No.: 104209-02-1
• Molecular Formula: C₂H₅F₃Ge
• Molecular Weight: 158.647
• Mol file: 104209-02-1.mol

Synonyms:

Chemical Property of (CF₃)GeH₂(CH₃)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (CF₃)GeH₂(CH₃)

There total 2 articles about (CF₃)GeH₂(CH₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

trifluoromethylgermane (85906-84-9) → (CF3)GeH2(CH3) (104209-02-1) + CF3GeH2I (85906-47-4) + (CF3)GeH(CH3)2 (104209-03-2) + Trifluormethyl-trimethylgermanium (21907-59-5) + perfluormethylgermanium iodide (1512-08-9)

Guidance literature:

With CH₃I; dimethyl zinc; In neat (no solvent); byproducts: CH3ZnI, CH4; (CH3)2Zn and CH3I condensed with excess CF3GeH3, mixt. warmed to room temp.; fractional condensation of volatile materials, further products; Kinetics;

DOI:10.1016/0022-328X(86)84031-1

Reference yield:

trifluoromethylgermane (85906-84-9) → (CF3)GeH2(CH3) (104209-02-1) + (CF3)GeH(CH3)2 (104209-03-2) + Trifluormethyl-trimethylgermanium (21907-59-5)

Guidance literature:

With CH₃I; dimethyl zinc; In neat (no solvent); byproducts: CH4, CH3ZnI; excess (CH3)2Zn and CH3I condensed with CF3GeH3, mixt. warmed to room temp. (sepn. of white solid); fractional condensation of volatile materials, unreacted (CF3)GeH3 and Me2Zn also present;

DOI:10.1016/0022-328X(86)84031-1

upstream raw materials:

trifluoromethylgermane

Refernces