1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol

Base Information

Chemical Name:1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol
CAS No.:199928-99-9
Molecular Formula:C₂₆H₂₆N₆O₄S₃
Molecular Weight:582.728
Hs Code.:

1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol

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Chemical Property of 1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol

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Technology Process of 1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol

There total 3 articles about 1-{[(5-{[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-1-yl)-2-oxoethyl]sulfanyl}-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-3-methyl-5-phenyl-4,5-dihydro-1H-pyrazol-5-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 93-91-4
1-phenylbutan-1,3-dione

: 75646-25-2
2,5-bis (mercaptoacetichydrazide)-1,3,4-thiadiazole

: 199928-99-9
1-(5-Hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-{5-[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-oxo-ethylsulfanyl]-[1,3,4]thiadiazol-2-ylsulfanyl}-ethanone

Guidance literature:: In 1,4-dioxane; water; at 85 ℃; for 3h;
DOI:10.1007/BF02290758

Reference yield:

: 75646-23-0
2,2'-[1,3,4-thiadiazole-2,5-diylbis(thio)]diacetic acid dimethyl ester

: 199928-99-9
1-(5-Hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-{5-[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-oxo-ethylsulfanyl]-[1,3,4]thiadiazol-2-ylsulfanyl}-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NH₂NH₂*H₂O / propan-2-ol / 30 - 40 °C

2: 62 percent / H₂O; dioxane / 3 h / 85 °C

With hydrazine hydrate; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1007/BF02290758

Reference yield:

: 75646-24-1
diethyl 2,2`-(1,3,4-thiadiazole-2,5-diyl)bis(sulfanediyl)diacetate

: 199928-99-9
1-(5-Hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-{5-[2-(5-hydroxy-3-methyl-5-phenyl-4,5-dihydro-pyrazol-1-yl)-2-oxo-ethylsulfanyl]-[1,3,4]thiadiazol-2-ylsulfanyl}-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / NH₂NH₂*H₂O / propan-2-ol / 30 - 40 °C

2: 62 percent / H₂O; dioxane / 3 h / 85 °C

With hydrazine hydrate; In 1,4-dioxane; water; isopropyl alcohol;
DOI:10.1007/BF02290758