η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

Base Information

Chemical Name:η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene
CAS No.:192438-32-7
Molecular Formula:C₃₅H₃₁Co
Molecular Weight:510.624
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

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Technology Process of η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

There total 1 articles about η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 22516-13-8
5-ethylcyclopentadiene

: 7440-48-4
cobalt

: 501-65-5
diphenyl acetylene

: 192438-32-7,137736-80-2
η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

Guidance literature:: In acetonitrile; Electrolysis; Ar-atmosphere; Co-anode, Fe-cathode, 0.1 M Bu4NCl or Bu4NBr, 0.5% water,2.5-10 mA/cm**2; water addn., extn. into hexane, drying (MgSO4), solvent removal, chromy.(SiO2, hexane/C6H6=1:1), evapn. (reduced pressure), drying (vac.); elem . anal.;
DOI:10.1016/S0022-328X(96)06693-4

Reference yield: 72.0%

: 192438-32-7,137736-80-2
η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

: 7553-56-2,12190-71-5,8031-47-8
iodine

: 603-35-0
triphenylphosphine

: 137736-83-5
η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide

Guidance literature:: In benzene; Ar-atmosphere; stirring equimolar amts. for 2 h; filtration, concn. (vac.), pptn. on pentane addn., collection (filtration), washing (pentane), drying (vac.), repeated pptn. from C6H6; elem. anal.;
DOI:10.1016/S0022-328X(96)06693-4