η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide

Base Information

• Chemical Name: η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide
• CAS No.: 137736-83-5
• Molecular Formula: C₂₅H₂₄CoI₂P
• Molecular Weight: 668.242
• Mol file: 137736-83-5.mol

Synonyms:

Chemical Property of η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide

There total 1 articles about η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene (192438-32-7,137736-80-2) + iodine (7553-56-2,12190-71-5,8031-47-8) + triphenylphosphine (603-35-0) → η(5)-ethylcyclopentadienyl(triphenylphosphine)cobalt diiodide (137736-83-5)

Guidance literature:

In benzene; Ar-atmosphere; stirring equimolar amts. for 2 h; filtration, concn. (vac.), pptn. on pentane addn., collection (filtration), washing (pentane), drying (vac.), repeated pptn. from C6H6; elem. anal.;

DOI:10.1016/S0022-328X(96)06693-4

upstream raw materials:

η(5)-ethylcyclopentadienylcobalt-η(4)-tetraphenylbutadiene

iodine

triphenylphosphine