Technology Process of C8H8N2O
There total 1 articles about C8H8N2O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(l) iodide; triethylamine;
bis-triphenylphosphine-palladium(II) chloride;
at 20 - 50 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium on activated carbon / ethanol; ethyl acetate / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -42 - 42 °C
2.2: 2.5 h / 20 - 42 °C
3.1: tetrahydrofuran / 2 h / -78 - 20 °C
4.1: Dess-Martin periodane / dichloromethane / 0.75 h / 20 °C
4.2: 0.17 h / 20 °C
With
oxalyl dichloride; hydrogen; Dess-Martin periodane; dimethyl sulfoxide;
palladium on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
2.1: Swern Oxidation / 2.2: Swern Oxidation / 4.1: Jones Oxidation;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen / palladium on activated carbon / ethanol; ethyl acetate / 20 °C
2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -42 - 42 °C
2.2: 2.5 h / 20 - 42 °C
3.1: tetrahydrofuran / 2 h / -78 - 20 °C
With
oxalyl dichloride; hydrogen; dimethyl sulfoxide;
palladium on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; ethyl acetate;
2.1: Swern Oxidation / 2.2: Swern Oxidation;