C₆₀H₆₀O₁₀S

Base Information

Chemical Name:C₆₀H₆₀O₁₀S
CAS No.:1404095-79-9
Molecular Formula:C₆₀H₆₀O₁₀S
Molecular Weight:973.196
Hs Code.:

C<sub>60</sub>H<sub>60</sub>O<sub>10</sub>S

Synonyms:

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Chemical Property of C₆₀H₆₀O₁₀S

Chemical Property:

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Technology Process of C₆₀H₆₀O₁₀S

There total 3 articles about C₆₀H₆₀O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127299-77-8
phenyl 3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1404095-79-9
C₆₀H₆₀O₁₀S

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

2.1: sodium; methanol / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

2.2: Amberlite IR-120 (H⁺)

3.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.75 h / -78 - 0 °C / Inert atmosphere

3.2: 0 °C / Inert atmosphere

With methanol; oxalyl dichloride; sodium; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 3.1: |Swern Oxidation / 3.2: |Swern Oxidation;
DOI:10.1039/c2ob26355f

Reference yield:

: 138181-67-6,127299-78-9
phenyl 2-O-acetyl-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1404095-79-9
C₆₀H₆₀O₁₀S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / methanol; tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

1.2: Amberlite IR-120 (H⁺)

2.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere; Molecular sieve

2.2: 0.75 h / -40 °C / Inert atmosphere; Molecular sieve

3.1: sodium; methanol / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

3.2: Amberlite IR-120 (H⁺)

4.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.75 h / -78 - 0 °C / Inert atmosphere

4.2: 0 °C / Inert atmosphere

With methanol; oxalyl dichloride; sodium methylate; sodium; dimethyl sulfoxide; In tetrahydrofuran; methanol; dichloromethane; 4.1: |Swern Oxidation / 4.2: |Swern Oxidation;
DOI:10.1039/c2ob26355f

Reference yield:

: 1404095-53-9
phenyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-glucopyranosyl-(1→2)-3,4,6-tri-O-benzyl-1-thio-α-D-mannopyranoside

: 1404095-79-9
C₆₀H₆₀O₁₀S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium; methanol / tetrahydrofuran / 48 h / 20 °C / Inert atmosphere

1.2: Amberlite IR-120 (H⁺)

2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.75 h / -78 - 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

With methanol; oxalyl dichloride; sodium; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1039/c2ob26355f