Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆

Base Information

Chemical Name:Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆
CAS No.:75070-58-5
Molecular Formula:C₄₃H₃₉O₂P₃Rh*F₆P
Molecular Weight:928.572
Hs Code.:

Rh(CO)2(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup> = Rh(CO)2(CH<sub>3</sub>C(CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)PF<sub>6</sub>

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Suppliers and Price of Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆

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Chemical Property of Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆

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Technology Process of Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆

There total 3 articles about Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)⁽¹⁺⁾*PF₆^(1-) = Rh(CO)2(CH₃C(CH₂P(C₆H₅)2)3)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: hexafluorophosphoric acid

: 124223-20-7,101075-59-6
[(CH₃C(CH₂PPh₂)3)Rh(CO)(H)]

: 75070-58-5
{Rh(CO)2(triphos)}PF₆

Guidance literature:: With CO; In methanol; water; addn. of Rh compound to a methanol soln. of HPF6 saturated with CO; CO is bubbled through the soln. for 30 min; pptn. (-10°C for 8 h);; filtration; washing with ether; drying under high-vac.; elem. anal.;;
DOI:10.1016/0022-328X(85)80205-9

Reference yield: 15.0%

: 60969-19-9
thallium(I) hexafluorophosphate

: {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(C₄H₄)}*(CH₃)2CO

: 75070-58-5
{Rh(CO)2(triphos)}PF₆

: 132296-97-0
{(CH₃C(CH₂P(C₆H₅)2)3)Rh(C₄H₄CO)}⁽¹⁺⁾*PF₆^(1-) = {(CH₃C(CH₂P(C₆H₅)2)3)Rh(C₄H₄CO)}(PF₆)

Guidance literature:: With CO; In tetrahydrofuran; byproducts: Cl(1-); treated a soln. of Rh-complex with TlPF6 under CO at 0°C for 40 min; added n-heptane; concentrated under N2; recrystd. from CH2Cl2/ethanol; elem. anal.;
DOI:10.1021/om00049a024

Reference yield:

: 121374-19-4
{RhH₂(CO)(triphos)}PF₆

: 75070-58-5
{Rh(CO)2(triphos)}PF₆

Guidance literature:: With carbon monoxide; In tetrahydrofuran; byproducts: H2; CO bubbled through soln. of complex (N2, room temp., 5 min); detn. by IR;
DOI:10.1021/om00110a011