Technology Process of C18H19BrO3
There total 5 articles about C18H19BrO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
acetonitrile;
for 6h;
Inert atmosphere;
Reflux;
DOI:10.1021/ja211305j
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium chlorite; aminosulfonic acid; sodium acetate / 1,4-dioxane; water; dimethyl sulfoxide / 0.75 h / 20 °C / Inert atmosphere
2: potassium carbonate / acetonitrile / 6 h / Inert atmosphere; Reflux
With
sodium chlorite; aminosulfonic acid; sodium acetate; potassium carbonate;
In
1,4-dioxane; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja211305j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: boron tribromide / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere
2: potassium carbonate / N,N-dimethyl-formamide / 15 h / 100 °C / Inert atmosphere
3: sodium chlorite; aminosulfonic acid; sodium acetate / 1,4-dioxane; water; dimethyl sulfoxide / 0.75 h / 20 °C / Inert atmosphere
4: potassium carbonate / acetonitrile / 6 h / Inert atmosphere; Reflux
With
sodium chlorite; aminosulfonic acid; sodium acetate; boron tribromide; potassium carbonate;
In
1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja211305j