[Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n

Base Information

• Chemical Name: [Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n
• CAS No.: 953776-75-5
• Molecular Formula: C₇H₄O₆S*C₁₀H₈N₂*Cd
• Molecular Weight: 484.768

Synonyms:

Chemical Property of [Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n

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Technology Process of [Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n

There total 1 articles about [Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

[2,2]bipyridinyl (366-18-7) + cadmium sulfate octahydrate + 5-sulfosalicilic acid dihydrate + potassium hydroxide → [Cd(5-sulfosalycilic acid-2H)(2,2'-bipyridine)]n (953776-75-5)

Guidance literature:

In water; High Pressure; 1 equiv. of metal-salt, 1 equiv. of sulfonic acid, 1 equiv. of N-base and 2.8 equiv. of KOH were stirred in H2O at room temp. for 30 min (pH=7-7.5), teflon-lined stainless steel reactor, heating at 150 °C for 72 h; cooling to room temp., crystals were filtered off, washed with H2O, elem. anal.;

DOI:10.1016/j.poly.2007.05.037

upstream raw materials:

[2,2]bipyridinyl

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