Technology Process of C28H32N2O13S
There total 4 articles about C28H32N2O13S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium methylate;
In
methanol;
at 20 ℃;
pH=8;
Inert atmosphere;
DOI:10.1039/c0nj00277a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetra-(n-butyl)ammonium iodide / methanol / 7 h / Inert atmosphere; Reflux
2: pyridine / 16 h / 20 °C / Inert atmosphere
3: pyridine; N-chloro-succinimide / chloroform / 0 - 25 °C / Inert atmosphere
4: sodium methylate / methanol / 20 °C / pH 8 / Inert atmosphere
With
pyridine; N-chloro-succinimide; sodium methylate; tetra-(n-butyl)ammonium iodide;
In
methanol; chloroform;
DOI:10.1039/c0nj00277a
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridine; N-chloro-succinimide / chloroform / 0 - 25 °C / Inert atmosphere
2: sodium methylate / methanol / 20 °C / pH 8 / Inert atmosphere
With
pyridine; N-chloro-succinimide; sodium methylate;
In
methanol; chloroform;
DOI:10.1039/c0nj00277a