2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine

Base Information

• Chemical Name: 2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine
• CAS No.: 1218917-35-1
• Molecular Formula: C₅₈H₈₈N₇O₈PS₂Si₂
• Molecular Weight: 1162.66

Synonyms:

Chemical Property of 2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine

Chemical Property:

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Technology Process of 2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine

There total 1 articles about 2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

2'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-guanosine (1218917-33-9) + N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) → 2'-O-(tert-butyldimethylsilyl)-5'-O-(4,4'-dimethoxytrityl)-N2-(tert-butyldithiopropyl)-O6-(trimethylsilylethyl)-3'-O-[(2-cyanoethoxy)-(N,N-diisopropylamino)]phosphinyl guanosine (1218917-35-1)

Guidance literature:

With pyridinium trifluroacetate; In dichloromethane; for 4h; Inert atmosphere; Cooling with ice;

DOI:10.1080/15257770903368385

upstream raw materials:

2'-O-tert-butyldimethylsilyl-5'-O-(4,4'-dimethoxytrityl)-N₂-(tert-butyldithiopropyl)-O₆-(trimethylsilylethyl)-guanosine

N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

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