Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2

Base Information

Chemical Name:Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2
CAS No.:270252-23-8
Molecular Formula:C₅₂H₄₀ClNOP₂Ru
Molecular Weight:893.366
Hs Code.:

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Chemical Property of Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2

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Technology Process of Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2

There total 1 articles about Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 157072-60-1,61521-25-3,166941-05-5,16971-33-8
(carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II)

: bis(2-(1'-naphthyl)pyridine)mercury

: 270252-23-8
Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2

Guidance literature:: In toluene; byproducts: Hg; mixt. in deoxygenated toluene was heated under reflux under N2 atm. for2 h; chromy. on silica gel column, hexane, CH2Cl2 as eluent; EtOH was added,reduced in vol. (vac.), crystals were filtered; elem. anal.;
DOI:10.1016/S0022-328X(99)00724-X

Reference yield: 82.0%

: 270252-23-8
Ru(η2-C,N-(2-(1'-naphthyl)pyridine))Cl(CO)(PPh3)2

: 128-04-1
sodium dimethyldithiocarbamate

: Ru(η2-C,N-(2-(1'-naphthyl)pyridine))(η2-dithiocarbamate)(CO)(PPh3) * 1/6 CH2Cl2

Guidance literature:: With AgSbF₆; In ethanol; dichloromethane; water; to a soln. of complex in CH2Cl2 was added AgSbF6 in H2O-EtOH, the soln.was stirred for 10 min, excess of H2O was added, org. layer collected, NaS2CNMe2 in H2O-EtOH was added, the soln. was stirred for 10 min; the organic layer was sepd., filtered, heated under reflux for 10 min, heptane was added, reduced in vol. (vac.), filtered; elem. anal.;
DOI:10.1016/S0022-328X(99)00724-X