Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl-

Base Information

Chemical Name:Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl-
CAS No.:13892-12-1
Molecular Formula:C26H26Ge2
Molecular Weight:483.672
Hs Code.:
Mol file:13892-12-1.mol

Synonyms:

Suppliers and Price of Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl-

There total 13 articles about Digermane, 1,2-dimethyl-1,1,2,2-tetraphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 27663-93-0
bromomethyldiphenylgermane

: 13892-12-1
1,2-dimethyl-1,1,2,2-tetraphenylgermane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; (Ar); soln. of SmI2 (2 equiv.) in THF was added to soln. of MePh2GeBr inhexamethylphosphoric triamide; mixt. was stirred at room temp. for 1 h; chromd. (silica gel, ether); evapd.; chromd. (silica gel, hexane);
DOI:10.1016/j.jorganchem.2004.12.032

Reference yield: 97.0%

: cis-bis(methyldiphenylgermyl)bis(dimethylphenylphosphine)platinum(II)

: 13892-12-1
1,2-dimethyl-1,1,2,2-tetraphenylgermane

Guidance literature:: With PPh₃; In benzene-d6; heating in a sealed tube at 120°C for 5 h in the presence of 5 mol equiv. of PPh3; monitored by NMR;
DOI:10.1246/bcsj.74.123

Reference yield: 95.0%

: 115514-17-5
methyldiphenylgermanium chloride

: 13892-12-1
1,2-dimethyl-1,1,2,2-tetraphenylgermane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; (Ar); soln. of SmI2 (2 equiv.) in THF was added to soln. of MePh2GeCl inhexamethylphosphoric triamide; mixt. was stirred at room temp. for 12 h; chromd. (silica gel, ether); evapd.; chromd. (silica gel, hexane);
DOI:10.1016/j.jorganchem.2004.12.032