6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

Base Information

Chemical Name:6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide
CAS No.:114660-19-4
Molecular Formula:C₃₀H₃₃N₄PS
Molecular Weight:512.659
Hs Code.:

6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<d,g><1,3,2>diazaphosphocine 6-sulphide

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Chemical Property of 6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

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Technology Process of 6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

There total 3 articles about 6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 27675-32-7
4,4'-dimethyl-2,2'-methylenedianiline

: 114660-19-4
6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

: 114681-19-5
C₄₅H₄₈N₆P₂S₂

Guidance literature:: With triethylamine; In benzene; 1.) 0 deg C; 2.) reflux, 3 h;

Reference yield:

: 73086-50-7
2-amino-5-methyl-N-tolylbenzylamine

: 114660-19-4
6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / H⁺ / 130 °C

2: 16 percent / triethylamine / benzene / 1.) 0 deg C; 2.) reflux, 3 h

With hydrogen cation; triethylamine; In benzene;

Reference yield:

: 17450-22-5
bis(4-methylphenylamino)methane

: 114660-19-4
6-<2-<2-amino-5-methylbenzyl>-4-methylanilino>-5,6,7,12-tetrahydro-2,10-dimethyldibenzo<1,3,2>diazaphosphocine 6-sulphide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / H⁺ / 70 °C

2: 65 percent / H⁺ / 130 °C

3: 16 percent / triethylamine / benzene / 1.) 0 deg C; 2.) reflux, 3 h

With hydrogen cation; triethylamine; In benzene;