Technology Process of Benzeneacetaldehyde, a-phenyl-a-2-propynyl-
There total 3 articles about Benzeneacetaldehyde, a-phenyl-a-2-propynyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 40 - 45 ℃;
for 2h;
DOI:10.1248/cpb.44.1858
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 85 percent / tetrabutylammonium hydrogen sulfate, aq. NaOH / 6 h / Ambient temperature
2: 91 percent / LiAlH4 / tetrahydrofuran / 2 h / 40 - 45 °C
With
sodium hydroxide; lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate;
In
tetrahydrofuran;
DOI:10.1248/cpb.44.1858
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C
1.2: 20 °C
2.1: diisobutylaluminium hydride / toluene; hexane / -78 - 20 °C / Inert atmosphere
With
sodium hydride; diisobutylaluminium hydride;
In
tetrahydrofuran; hexane; toluene; mineral oil;
DOI:10.1002/chem.201404987
