Ru(C_.ident.CSi(i)Pr₃)(PPh₃)2Cp

Base Information

• Chemical Name: Ru(C_.ident.CSi(i)Pr₃)(PPh₃)2Cp
• CAS No.: 1092837-05-2
• Molecular Formula: C₅₂H₅₆P₂RuSi
• Molecular Weight: 872.12
• Mol file: 1092837-05-2.mol

Synonyms:

Chemical Property of Ru(C_.ident.CSi(i)Pr₃)(PPh₃)2Cp

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Ru(C_.ident.CSi(i)Pr₃)(PPh₃)2Cp

There total 1 articles about Ru(C_.ident.CSi(i)Pr₃)(PPh₃)2Cp which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) (32993-05-8) + tris-iso-propylsilyl acetylene (89343-06-6) → Ru(C.ident.CSi(i)Pr3)(PPh3)2Cp (1092837-05-2)

Guidance literature:

With NaOCH₃; In methanol; under N2; mixt. of ruthenium complex and alkyne in MeOH refluxed for 2 h, cooled, 1 M soln. of NaOMe in MeOH added, stirred at room temp. for 30min; partly evapd. under vac., ppt. filtered off, washed with cold MeOH, dried; elem. anal.;

DOI:10.1016/j.jorganchem.2008.07.006

upstream raw materials:

chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II)

tris-iso-propylsilyl acetylene