C₃₁H₂₇BF₂N₂

Base Information

• Chemical Name: C₃₁H₂₇BF₂N₂
• CAS No.: 1359876-86-0
• Molecular Formula: C₃₁H₂₇BF₂N₂
• Molecular Weight: 476.377
• Mol file: 1359876-86-0.mol

Synonyms:

Chemical Property of C₃₁H₂₇BF₂N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₂₇BF₂N₂

There total 3 articles about C₃₁H₂₇BF₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dimethyl-1H-pyrrole (625-82-1) → C31H27BF2N2 (1359876-86-0)

Guidance literature:

Multi-step reaction with 4 steps

1: dichloromethane / 20 °C / Inert atmosphere

2: boron trifluoride diethyl etherate; triethylamine / dichloromethane / Cooling with ice; Inert atmosphere

3: N-iodo-succinimide / dichloromethane / 2 h

4: potassium phosphate tribasic trihydrate; palladium diacetate / ethanol; toluene / 8 h / 80 °C / Inert atmosphere

With N-iodo-succinimide; potassium phosphate tribasic trihydrate; boron trifluoride diethyl etherate; palladium diacetate; triethylamine; In ethanol; dichloromethane; toluene; 4: Suzuki coupling;

DOI:10.1021/jo202215x

Reference yield:

3,3',5,5'-tetramethyl-6-phenylpyrromethene (680222-61-1) → C31H27BF2N2 (1359876-86-0)

Guidance literature:

Multi-step reaction with 3 steps

1: boron trifluoride diethyl etherate; triethylamine / dichloromethane / Cooling with ice; Inert atmosphere

2: N-iodo-succinimide / dichloromethane / 2 h

3: potassium phosphate tribasic trihydrate; palladium diacetate / ethanol; toluene / 8 h / 80 °C / Inert atmosphere

With N-iodo-succinimide; potassium phosphate tribasic trihydrate; boron trifluoride diethyl etherate; palladium diacetate; triethylamine; In ethanol; dichloromethane; toluene; 3: Suzuki coupling;

DOI:10.1021/jo202215x

Reference yield:

phenyl BODIPY → C31H27BF2N2 (1359876-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: N-iodo-succinimide / dichloromethane / 2 h

2: potassium phosphate tribasic trihydrate; palladium diacetate / ethanol; toluene / 8 h / 80 °C / Inert atmosphere

With N-iodo-succinimide; potassium phosphate tribasic trihydrate; palladium diacetate; In ethanol; dichloromethane; toluene; 2: Suzuki coupling;

DOI:10.1021/jo202215x

upstream raw materials:

2,4-dimethyl-1H-pyrrole

3,3',5,5'-tetramethyl-6-phenylpyrromethene