Technology Process of 3-<3-<3-(formylamino)benzamido>benzamido>benzamidopropionamidine hydrochloride
There total 12 articles about 3-<3-<3-(formylamino)benzamido>benzamido>benzamidopropionamidine hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: SOCl2 / 4 h / Heating
2: 75 percent / 4percent NaHCO3 / acetone / 12 h / ice-bath
3: 92 percent / 50 percent methanolic 2 N NaOH / methanol / 2 h
4: SOCl2 / 4 h / Heating
5: 72 percent / 4 percent NaHCO3 / acetone / 12 h / Ambient temperature
6: 1) EtOH, HCl, 2) NH3 / 1) ice-bath, 1.5 h, 2) EtOH, 1 h
7: H2 / 10percent Pd-C / methanol
8: Ac2O
With
hydrogenchloride; sodium hydroxide; thionyl chloride; ethanol; ammonia; hydrogen; acetic anhydride; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; acetone;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 75 percent / 4percent NaHCO3 / acetone / 12 h / ice-bath
2: 92 percent / 50 percent methanolic 2 N NaOH / methanol / 2 h
3: SOCl2 / 4 h / Heating
4: 72 percent / 4 percent NaHCO3 / acetone / 12 h / Ambient temperature
5: 1) EtOH, HCl, 2) NH3 / 1) ice-bath, 1.5 h, 2) EtOH, 1 h
6: H2 / 10percent Pd-C / methanol
7: Ac2O
With
hydrogenchloride; sodium hydroxide; thionyl chloride; ethanol; ammonia; hydrogen; acetic anhydride; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; acetone;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2 / 4 h / Heating
2: 72 percent / 4 percent NaHCO3 / acetone / 12 h / Ambient temperature
3: 1) EtOH, HCl, 2) NH3 / 1) ice-bath, 1.5 h, 2) EtOH, 1 h
4: H2 / 10percent Pd-C / methanol
5: Ac2O
With
hydrogenchloride; thionyl chloride; ethanol; ammonia; hydrogen; acetic anhydride; sodium hydrogencarbonate;
palladium on activated charcoal;
In
methanol; acetone;
