Technology Process of 1,1-ethylenedioxy-4-hydroxy-4,5-bis-(p-methoxyphenyl)pentane
There total 1 articles about 1,1-ethylenedioxy-4-hydroxy-4,5-bis-(p-methoxyphenyl)pentane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
magnesium;
Yield given. Multistep reaction;
1.) tetahydrofuran, 30-35 deg C ,1 h, 2.) room temperature;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) hydrogen, 2.) hydrochloric acid / 10percent palladium-carbon / 1.) ethanol, 24 h, 2.) dioxan ,reflux, 1 h
2: 80 percent / silver nitrate, sodium hydroxide / ethanol; H2O / 4 h / Ambient temperature
3: 42 percent / hydrogen fluoride / 48 h / Ambient temperature
4: 83 percent / lithium aluminium hydride / diethyl ether / 2 h / Ambient temperature
5: 85 percent / toluene-p-sulphonic acid / toluene / 3 h / Heating
With
hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen fluoride; hydrogen; toluene-4-sulfonic acid; silver nitrate;
palladium on activated charcoal;
In
diethyl ether; ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) hydrogen, 2.) hydrochloric acid / 10percent palladium-carbon / 1.) ethanol, 24 h, 2.) dioxan ,reflux, 1 h
2: 80 percent / silver nitrate, sodium hydroxide / ethanol; H2O / 4 h / Ambient temperature
3: 42 percent / hydrogen fluoride / 48 h / Ambient temperature
With
hydrogenchloride; sodium hydroxide; hydrogen fluoride; hydrogen; silver nitrate;
palladium on activated charcoal;
In
ethanol; water;