3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Base Information

Chemical Name:3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
CAS No.:75415-42-8
Molecular Formula:C₃₆H₅₃IO₄
Molecular Weight:676.719
Hs Code.:

3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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Chemical Property of 3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

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Technology Process of 3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

There total 1 articles about 3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26358-65-6
5α-cholestane-3β,6β-diol 6-acetate

: 618-51-9
3-Iodobenzoic acid

: 75415-42-8
3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 15h;

Reference yield:

: 75415-42-8
3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

: 75415-49-5
9,10-seco-1,3,5⁽¹⁰⁾-cholestatrien-9-one

Guidance literature:: Multi-step reaction with 10 steps

1: 2.) KOH / 1.) chlorination, 2.) H₂O, EtOH

2: 11 g / pyridine / 16 h / 25 °C

3: 5.9 g / phosphoryl chloride, pyridine / 20 h / 20 °C

4: 3.2 g / KOH / methanol; benzene / 12 h / 20 °C

5: Jones reagent / acetone / 0.17 h

6: H₂SO₄ / acetone / 16 h

7: 500 mg / dichlorodicyanobenzoquinone / benzene / 24 h / Heating

8: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

9: 190 mg / LiAlH₄ / tetrahydrofuran / 16 h / Heating

10: pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; jones reagent; sulfuric acid; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; acetone; benzene;

Reference yield:

: 75415-42-8
3-Iodo-benzoic acid (3R,5S,6R,8S,9S,10R,13R,14S,17R)-6-acetoxy-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester

: 75415-52-0
C₂₉H₄₆S₂

Guidance literature:: Multi-step reaction with 11 steps

1: 2.) KOH / 1.) chlorination, 2.) H₂O, EtOH

2: 11 g / pyridine / 16 h / 25 °C

3: 5.9 g / phosphoryl chloride, pyridine / 20 h / 20 °C

4: 3.2 g / KOH / methanol; benzene / 12 h / 20 °C

5: Jones reagent / acetone / 0.17 h

6: H₂SO₄ / acetone / 16 h

7: 500 mg / dichlorodicyanobenzoquinone / benzene / 24 h / Heating

8: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

9: 190 mg / LiAlH₄ / tetrahydrofuran / 16 h / Heating

10: pyridinium chlorochromate / CH₂Cl₂ / Ambient temperature

11: 140 mg / boron trifluoride etherate / acetic acid

With pyridine; potassium hydroxide; lithium aluminium tetrahydride; jones reagent; sulfuric acid; boron trifluoride diethyl etherate; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In tetrahydrofuran; methanol; dichloromethane; acetic acid; acetone; benzene;