diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate

Base Information

Chemical Name:diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate
CAS No.:104051-71-0
Molecular Formula:C₁₀H₁₄O₂V*2C₁₂H₁₀O₄P
Molecular Weight:715.527
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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate

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Technology Process of diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate

There total 1 articles about diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 838-85-7
diphenyl hydrogen phosphate

: 12083-48-6
bis(cyclopentadienyl)vanadium dichloride

: 104051-71-0
diaquabis(cyclopentadienyl)vanadium(IV) diphenyl phosphate

Guidance literature:: In water; byproducts: HCl; (N2); dissolving (C5H5)2VCl2 at room temp. im doubly distd. deionized H2O and stirring for 1 h; filtration; layering the filtrate onto a previously filtered aq. soln. of diphenyl phosphate (satd. with N2); standing overnight; decanting the aq. soln.; washing the crystals 3 times (min. amt. of ice-cold H2O, N2); drying in vac.; elem. anal.;
DOI:10.1021/ja00283a022