C₅₄H₇₆O₆Si₂

Base Information

Chemical Name:C₅₄H₇₆O₆Si₂
CAS No.:956223-80-6
Molecular Formula:C₅₄H₇₆O₆Si₂
Molecular Weight:877.365
Hs Code.:

C<sub>54</sub>H<sub>76</sub>O<sub>6</sub>Si<sub>2</sub>

Synonyms:

Suppliers and Price of C₅₄H₇₆O₆Si₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₄H₇₆O₆Si₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₄H₇₆O₆Si₂

There total 22 articles about C₅₄H₇₆O₆Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₇H₇₀O₆Si₂

: 100-39-0
benzyl bromide

: 956223-80-6
C₅₄H₇₆O₆Si₂

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃;
DOI:10.1055/s-2007-985585

Reference yield:

: 869487-89-8
(S)-3-methyl-6-(trimethylsilyl)hex-5-ynal

: 956223-80-6
C₅₄H₇₆O₆Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: n-BuLi / -78 °C

2: Dess-Martin periodinane; NaHCO₃ / 0 - 20 °C

3: 96 percent / i-Pr₂NEt; LiCl / acetonitrile / 20 °C

4: 92 percent / AD-mix α; MeSO2NH2; NaHCO3 / 2-methyl-propan-2-ol; H2O / 0 °C

5: 95 percent / PPTS / CH₂Cl₂ / 0 - 20 °C

6: K-selectride / tetrahydrofuran / -78 °C

7: NaHMDS / tetrahydrofuran; dimethylformamide / 0 °C

With AD-mix-α; n-butyllithium; methanesulfonamide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; lithium chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 4: Sharpless asymmetric dihydroxylation;
DOI:10.1055/s-2007-985585

Reference yield:

: (R)-2-(dichloromethylene)-4-methyltetrahydro-2H-pyran

: 956223-80-6
C₅₄H₇₆O₆Si₂

Guidance literature:: Multi-step reaction with 12 steps

1: Li / tetrahydrofuran / Heating

2: PPTS / CH₂Cl₂ / 0 - 20 °C

3: n-BuLi / tetrahydrofuran / -78 °C

4: PPTS / methanol / 0 - 20 °C

5: 2-iodoxybenzoic acid / CH₂Cl₂; dimethylsulfoxide / 20 °C

6: n-BuLi / -78 °C

7: Dess-Martin periodinane; NaHCO₃ / 0 - 20 °C

8: 96 percent / i-Pr₂NEt; LiCl / acetonitrile / 20 °C

9: 92 percent / AD-mix α; MeSO2NH2; NaHCO3 / 2-methyl-propan-2-ol; H2O / 0 °C

10: 95 percent / PPTS / CH₂Cl₂ / 0 - 20 °C

11: K-selectride / tetrahydrofuran / -78 °C

12: NaHMDS / tetrahydrofuran; dimethylformamide / 0 °C

With AD-mix-α; n-butyllithium; methanesulfonamide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; lithium; sodium hydrogencarbonate; potassium tri-sec-butyl-borohydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol; 9: Sharpless asymmetric dihydroxylation;
DOI:10.1055/s-2007-985585