C₂₃H₃₁NO₁₀

Base Information

Chemical Name:C₂₃H₃₁NO₁₀
CAS No.:1027139-76-9
Molecular Formula:C₂₃H₃₁NO₁₀
Molecular Weight:481.5
Hs Code.:

C<sub>23</sub>H<sub>31</sub>NO<sub>10</sub>

Synonyms:

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Chemical Property of C₂₃H₃₁NO₁₀

Chemical Property:

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Technology Process of C₂₃H₃₁NO₁₀

There total 8 articles about C₂₃H₃₁NO₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6668-24-2,114764-47-5
2-methyl-1-phenyl-1,3-butanedione

: 1027139-76-9
C₂₃H₃₁NO₁₀

Guidance literature:: Multi-step reaction with 4 steps

1.1: formic acid; triethylamine / (S,S)-Ru-[N-(tosyl)-1,2-diphenylethylenediamine](p-cymene) / dichloromethane / 3 h / 40 °C

1.2: Zn(BH₄)2 / 2; 13 / 30 h / 0 °C

2.1: pyridine; dmap / 0.5 h / 20 °C

3.1: ruthenium trichloride; periodic acid / tetrachloromethane; water; acetonitrile / 18 h

4.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C

With pyridine; dmap; ruthenium trichloride; formic acid; benzotriazol-1-ol; periodic acid; triethylamine; dicyclohexyl-carbodiimide; (S,S)-Ru-[N-(tosyl)-1,2-diphenylethylenediamine](p-cymene); In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1021/jo050407s

Reference yield:

: 858132-52-2
(1R,2S,3R)-1,3-diacetoxy-2-methyl-1-phenylbutan

: 1027139-76-9
C₂₃H₃₁NO₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: ruthenium trichloride; periodic acid / tetrachloromethane; water; acetonitrile / 18 h

2: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C

With dmap; ruthenium trichloride; benzotriazol-1-ol; periodic acid; dicyclohexyl-carbodiimide; In tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1021/jo050407s

Reference yield:

: 1026913-67-6
C₂₆H₂₅NO₂

: 1027139-76-9
C₂₃H₃₁NO₁₀

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride

1.2: molecular sieves 4 Angstroem / 13 / 1 h / 20 °C

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / methanol; acetone; tert-butyl alcohol / 3 h / 20 °C

3.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C

4.1: sodium chlorite; potassium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 0.5 h / 20 °C

5.1: tert-butyl methyl ether; potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

6.1: trifluoroacetic acid / dichloromethane / 0.17 h / 20 °C

7.1: dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C

With dmap; sodium chlorite; sodium periodate; potassium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; tert-butyl methyl ether; sodium hydride; potassium carbonate; benzotriazol-1-ol; 4-methylmorpholine N-oxide; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; tert-butyl alcohol;
DOI:10.1021/jo050407s