4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

Base Information

Chemical Name:4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine
CAS No.:141859-20-3
Molecular Formula:C₃₁H₂₅Cl₃N₆S₂
Molecular Weight:652.071
Hs Code.:

4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

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Chemical Property of 4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

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Technology Process of 4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

There total 3 articles about 4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 141859-17-8
2,5-dihydro-5-(2-iminopropylidene)-2-<5-(3-methylisothiazolyl)>-1,2,4-thiadiazole

: 39887-78-0
N-methyl-p-chlorobenzimidoyl chloride

: 141859-20-3
4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

Guidance literature:: In acetonitrile; for 48h; Ambient temperature;

Reference yield: 3.0%

: 24340-76-9
3-methyl-5-aminothiazole

: 39887-78-0
N-methyl-p-chlorobenzimidoyl chloride

: 141859-17-8
2,5-dihydro-5-(2-iminopropylidene)-2-<5-(3-methylisothiazolyl)>-1,2,4-thiadiazole

: 141859-20-3
4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In acetonitrile; for 39h; Ambient temperature;

Reference yield:

: 39887-78-0
N-methyl-p-chlorobenzimidoyl chloride

: 141859-20-3
4-Chloro-N-[3-(4-chloro-phenyl)-2-[3-(4-chloro-phenyl)-2-(3-methyl-isothiazol-5-yl)-2H-[1,2,4]thiadiazol-(5E)-ylidene]-1-methyl-3-[(E)-methylimino]-prop-(E)-ylidene]-N'-methyl-benzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / 1,4-diazabicyclo<2.2.2>octane / acetonitrile / 39 h / Ambient temperature

2: 21 percent / acetonitrile / 48 h / Ambient temperature

With 1,4-diaza-bicyclo[2.2.2]octane; In acetonitrile;