3,5-Hexadienoic acid, 2-oxo-6-phenyl-, potassium salt

Base Information

Chemical Name:3,5-Hexadienoic acid, 2-oxo-6-phenyl-, potassium salt
CAS No.:139005-35-9
Molecular Formula:C₁₂H₉O₃*K
Molecular Weight:240.3
Hs Code.:
Mol file:139005-35-9.mol

Synonyms:

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Chemical Property of 3,5-Hexadienoic acid, 2-oxo-6-phenyl-, potassium salt

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Technology Process of 3,5-Hexadienoic acid, 2-oxo-6-phenyl-, potassium salt

There total 1 articles about 3,5-Hexadienoic acid, 2-oxo-6-phenyl-, potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127-17-3
2-oxo-propionic acid

: 104-55-2
3-phenyl-propenal

: 139005-35-9
C₁₂H₉O₃^(1-)*K⁽¹⁺⁾

Guidance literature:: With potassium hydroxide; In methanol; at 30 ℃; for 1h;
DOI:10.1002/chem.201303512

Reference yield:

: 139005-35-9
C₁₂H₉O₃^(1-)*K⁽¹⁺⁾

: 1-ethyl 6-isopropyl 2-nitro-5-oxo-3-((E)-styryl)hexanedioate

Guidance literature:: Multi-step reaction with 2 steps

1: acetyl chloride / 0 - 20 °C / Reflux

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 10 h / 20 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; In dichloromethane; 2: |Michael Addition;
DOI:10.1002/chem.201303512

Reference yield:

: 139005-35-9
C₁₂H₉O₃^(1-)*K⁽¹⁺⁾

: (3R)-1-ethyl 6-isopropyl 2-nitro-5-oxo-3-((E)-styryl)hexanedioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetyl chloride / 0 - 20 °C / Reflux

2.1: BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; lithium carbonate; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol / toluene / 1 h / 0 °C / Inert atmosphere

2.2: 0 °C / Inert atmosphere

With BF₄*C₈H₁₂CuN₄⁽¹⁺⁾; (S)-2-((2-(hydroxydi-p-tolylmethyl)pyrrolidin-1-yl)methyl)-6-(trifluoromethyl)phenol; lithium carbonate; acetyl chloride; In toluene; 2.1: |Michael Addition / 2.2: |Michael Addition;
DOI:10.1002/chem.201303512