4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

Base Information

Chemical Name:4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride
CAS No.:1026235-71-1
Molecular Formula:C₁₅H₁₃ClO₄
Molecular Weight:292.719
Hs Code.:

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Chemical Property of 4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

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Technology Process of 4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

There total 7 articles about 4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 958883-52-8
4-benzyloxy-3-hydroxy-5-methoxybenzoic acid

: 1026235-71-1
4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

Guidance literature:: With thionyl chloride; In toluene; for 2h; Heating;
DOI:10.1002/jlcr.1145

Reference yield:

: 852810-63-0
methyl 4-(benzyloxy)-3-hydroxy-5-methoxybenzoate

: 1026235-71-1
4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 82.4 percent / aqueous KOH / methanol / 1 h / Heating

2: thionyl chloride / toluene / 2 h / Heating

With potassium hydroxide; thionyl chloride; In methanol; toluene;
DOI:10.1002/jlcr.1145

Reference yield:

: 99-24-1
methyl galloate

: 1026235-71-1
4-benzyloxy-3-hydroxy-5-methoxybenzoyl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: 93 percent / pyridine / 2 h / 0 - 20 °C

2: 72 percent / potassium carbonate; potassium iodide / acetone / 18 h / Heating

3: 90 percent / potassium carbonate / methanol; H₂O / 0.33 h / 20 °C

4: 67.5 percent / potassium carbonate / dimethylformamide / 5 h / 20 °C

5: 82.4 percent / aqueous KOH / methanol / 1 h / Heating

6: thionyl chloride / toluene / 2 h / Heating

With potassium hydroxide; thionyl chloride; potassium carbonate; potassium iodide; In pyridine; methanol; water; N,N-dimethyl-formamide; acetone; toluene; 2: Williamson alkylation;
DOI:10.1002/jlcr.1145