(2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂

Base Information

Chemical Name:(2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂
CAS No.:455894-13-0
Molecular Formula:C₂₃H₂₃CdCl₂N₃
Molecular Weight:524.772
Hs Code.:

(2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl<sub>2</sub>

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Chemical Property of (2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂

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Technology Process of (2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂

There total 1 articles about (2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 221391-10-2
2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine

: 10108-64-2
cadmium(II) chloride

: 455894-13-0
(2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂

Guidance literature:: In butan-1-ol; (N2); standard Schlenk technique; 1-butanol was added via syringe to mixt. of CdCl2 (1 equiv.) and ligand (1 equiv.); soln. was stirred at 80°C for 0.5 h; solvent removed (vac.);
DOI:10.1016/S0020-1693(02)00735-1

Reference yield: 70.0%

: 455894-13-0
(2,6-bis[(2,6-dimethylphenylimino)methyl]pyridine)CdCl₂

: 148-18-5
sodium N,N-diethyldithiocarbamate

: 455894-22-1
[(2,6-bis((2,6-dimethylphenylimino)methyl)pyridine)Cd(S₂CNEt₂)][Cl]

Guidance literature:: In tetrahydrofuran; (N2); standard Schlenk technique; mixt. of Cd complex (1 equiv.) and ligand (1 equiv.) in THF was stirred for 4 h; solvent removed (vac.); residue extd. (toluene); filtered; evapd.;
DOI:10.1016/S0020-1693(02)00735-1