[As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)

Base Information

Chemical Name:[As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)
CAS No.:87196-85-8
Molecular Formula:C₂H₈CoN₁₄*C₂₄H₂₀As
Molecular Weight:670.517
Hs Code.:

[As(C<sub>6</sub>H<sub>5</sub>)4]<sup>(1+)</sup> tetrazidoethylenediaminecobaltate(III)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)

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Technology Process of [As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)

There total 2 articles about [As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: sodium azide

: 104170-16-3
tetraphenylarsonium chloride monohydrate

: Co⁽³⁺⁾*3Cl^(1-)*H₂O*H₂NCH₂CH₂NH₂=[CoCl₂(H₂O)(H₂NCH₂CH₂NH₂)]Cl

: 87196-85-8
[As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)

Guidance literature:: In water; acetic acid; addn. of HOAc, a soln. of AsPh4Cl*H2O and a soln. of NaN3 to a soln. of(CoCl2(H2O)en)Cl, standing for 1 h at room temp.; filtn., washing with water, drying in vacuo over P4O10, elem. anal.;

Reference yield: 74.0%

: sodium azide

: cobalt(II) chloride hexahydrate

: 104170-16-3
tetraphenylarsonium chloride monohydrate

: 333-18-6
1,2-diaminoethane dihydrochloride

: 87196-85-8
[As(C₆H₅)4]⁽¹⁺⁾ tetrazidoethylenediaminecobaltate(III)

Guidance literature:: With dihydrogen peroxide; In water; acetic acid; addn. of HOAc, a soln. of CoCl2*6H2O and H2O2 to a soln. of NaN3 with cooling, cooling for 10 min, addn. of a soln. of ethylenediammoniumchloride, keeping for 1 h at 50°C, standing overnight, filtn., addn. ofa soln. of AsPh4Cl*H2O with stirring; filtn., washing with water, drying in vacuo over P4O10;