C₅₅H₆₀N₁₈O₉

Base Information

Chemical Name:C₅₅H₆₀N₁₈O₉
CAS No.:915286-93-0
Molecular Formula:C₅₅H₆₀N₁₈O₉
Molecular Weight:1117.2
Hs Code.:

C<sub>55</sub>H<sub>60</sub>N<sub>18</sub>O<sub>9</sub>

Synonyms:

Suppliers and Price of C₅₅H₆₀N₁₈O₉

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₅₅H₆₀N₁₈O₉

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₅₅H₆₀N₁₈O₉

There total 17 articles about C₅₅H₆₀N₁₈O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915286-72-5
2-amino-4-chloro-7-[2'-deoxy-3',5'-di-O-(4-chlorobenzoyl)-β-D-erythro-pentofuranosyl]-7H-pyrrolo[2,3-d]pyrimidine

: 915286-93-0
C₅₅H₆₀N₁₈O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: 93 percent / Dowex 550A / 2 h / Heating

2.1: trimethylsilyl chloride; pyridine / 0.5 h

2.2: 70 percent / 6 h / 20 °C

3.1: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

4.1: 85 percent / ammonia / methanol / 1 h / 20 °C

5.1: 88 percent / pyridine; 4-dimethylaminopyridine / 15 h / 20 °C

6.1: 80 percent / lithium azide / dimethylformamide / 2 h / 90 °C

7.1: 96 percent / sodium thiocresolate / dimethylformamide / 1 h / 90 °C

8.1: 98 percent / hydrogen / palladium on carbon / ethanol / 5 h / 20 °C / 2327.17 Torr

9.1: 68 percent / diethylamine / CH₂Cl₂ / -40 - 20 °C

10.1: 76 percent / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; chloro-trimethyl-silane; lithium azide; sodium 4-mercaptobenzoate; di-isopropyl azodicarboxylate; DOWEX 550A; ammonia; hydrogen; diethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; 3.1: Mitsunobu reaction;
DOI:10.1016/j.bmc.2006.05.074

Reference yield:

: 915286-73-6
7-[2'-deoxy-3',5'-di-O-(4-nitrobenzoyl)-β-D-threo-pentofuranosyl]-2-isobutyrylamino-4-methoxy-7H-pyrrolo[2,3-d]pyrimidine

: 915286-93-0
C₅₅H₆₀N₁₈O₉

Guidance literature:: Multi-step reaction with 8 steps

1: 85 percent / ammonia / methanol / 1 h / 20 °C

2: 88 percent / pyridine; 4-dimethylaminopyridine / 15 h / 20 °C

3: 80 percent / lithium azide / dimethylformamide / 2 h / 90 °C

4: 96 percent / sodium thiocresolate / dimethylformamide / 1 h / 90 °C

5: 98 percent / hydrogen / palladium on carbon / ethanol / 5 h / 20 °C / 2327.17 Torr

6: 68 percent / diethylamine / CH₂Cl₂ / -40 - 20 °C

7: 76 percent / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; lithium azide; sodium 4-mercaptobenzoate; ammonia; hydrogen; diethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2006.05.074

Reference yield:

: 121150-07-0
7-(2'-deoxy-β-D-erythro-pentofuranosyl)-2-isobutyrylamino-4-methoxy-7H-pyrrolo[2,3-d]pyrimidine

: 915286-93-0
C₅₅H₆₀N₁₈O₉

Guidance literature:: Multi-step reaction with 9 steps

1: triphenylphosphine; diisopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C

2: 85 percent / ammonia / methanol / 1 h / 20 °C

3: 88 percent / pyridine; 4-dimethylaminopyridine / 15 h / 20 °C

4: 80 percent / lithium azide / dimethylformamide / 2 h / 90 °C

5: 96 percent / sodium thiocresolate / dimethylformamide / 1 h / 90 °C

6: 98 percent / hydrogen / palladium on carbon / ethanol / 5 h / 20 °C / 2327.17 Torr

7: 68 percent / diethylamine / CH₂Cl₂ / -40 - 20 °C

8: 76 percent / CH₂Cl₂ / 2 h / 20 °C

With pyridine; dmap; lithium azide; sodium 4-mercaptobenzoate; di-isopropyl azodicarboxylate; ammonia; hydrogen; diethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: Mitsunobu reaction;
DOI:10.1016/j.bmc.2006.05.074