1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene

Base Information

Chemical Name:1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene
CAS No.:1192236-53-5
Molecular Formula:C₂₂H₂₄FeN₂O
Molecular Weight:388.292
Hs Code.:

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Chemical Property of 1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene

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Technology Process of 1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene

There total 1 articles about 1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1192236-40-0
1-[(4-phenylpiperazin-1-yl)methyl]ferrocene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1192236-53-5
1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene

Guidance literature:: With n-butyllithium; water; In diethyl ether; hexane; (under Ar, in dark); Fe-complex in Et2O treated with butyllithium in hexane at room temp. with stirring for 16 h, treated with N,N-dimethylformamide at room temp. for 4 h, hydrolyzed with H2O; aq. phase washed with Et2O, dried over Na2SO4, concd., SiO2 column chromy. with Et2O/hexane;
DOI:10.1002/hlca.200800461

Reference yield: 21.0%

: 188290-36-0,8014-23-1,25233-34-5
thiophene

: 1192236-53-5
1-formyl-2-[(4-phenylpiperazin-1-yl)methyl]ferrocene

: 1192236-72-8
1,1''-[thiophene-2,5-diylbis(hydroxymethylene)]bis[2-[(4-phenylpiperazin-1-yl)methyl]ferrocene]

Guidance literature:: With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; ammonium chloride; In tetrahydrofuran; hexane; (under Ar, in dark); thiophene added to soln. of butyllithium and N,N,N',N'-tetramethylethane-1,2-diamine in hexane, refluxed for 2 h, cooled toroom temp., added dropwise to soln. of Fe-complex in THF at 0°C, warmed to room temp.; aq. NH4Cl added, aq. phase extd. with Et2O, organic phase washed with H2O, brine, dried over MgSO4, concd., SiO2 column chromy. with Et2O/hexane;
DOI:10.1002/hlca.200800461