[TiCl(N(CH₂CH(C₆H₅)O)3)]

Base Information

Chemical Name:[TiCl(N(CH₂CH(C₆H₅)O)3)]
CAS No.:766549-44-4
Molecular Formula:C₂₄H₂₄ClNO₃Ti
Molecular Weight:457.792
Hs Code.:

[TiCl(N(CH<sub>2</sub>CH(C<sub>6</sub>H<sub>5</sub>)O)3)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [TiCl(N(CH₂CH(C₆H₅)O)3)]

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Technology Process of [TiCl(N(CH₂CH(C₆H₅)O)3)]

There total 1 articles about [TiCl(N(CH₂CH(C₆H₅)O)3)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 767356-71-8,191410-20-5,193023-73-3,1219115-01-1,1219115-02-2,1219115-03-3
[((CH₃)2CHO)Ti(N(CH₂CH(C₆H₅)O)3)]

: 75-36-5
acetyl chloride

: 766549-44-4,918632-24-3
[TiCl(N(CH₂CH(C₆H₅)O)3)]

Guidance literature:: In toluene; (Ar); Schlenk technique; CH3C(O)Cl was added to soln. of Ti complex in toluene; mixt. was stirred at room temp. for 2 h; hexane added; solvent removed; residue redissolved in CH2Cl2; hexane added; solvent removed; dried (vac.); elem. anal.;
DOI:10.1021/om034408r

Reference yield: 55.0%

: 766549-44-4,918632-24-3
[TiCl(N(CH₂CH(C₆H₅)O)3)]

: 7732-18-5
water

: [Ti2(N(CH2CH(C6H5)O)3)2(μ3-O)]2

Guidance literature:: In water; toluene; (Ar); Schlenk technique; mixt. of Ti complex in toluene and distd. H2O (0.5 equiv.) was stirred at room temp. for 30 min; toluene distd. (vac.); elem. anal.;
DOI:10.1021/om034408r