5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

Base Information

Chemical Name:5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin
CAS No.:1430198-57-4
Molecular Formula:C₄₀H₂₁F₁₀N₅O₂
Molecular Weight:793.623
Hs Code.:

Synonyms:

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Chemical Property of 5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

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Technology Process of 5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

There total 4 articles about 5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 873840-21-2
(5-{1-[5-(hydroxy-pentafluorophenyl-methyl)-1H-pyrrol-2-yl]-1-methyl-ethyl}-1H-pyrrol-2-yl)-pentafluorophenyl-methanol

: 143859-77-2
2,2'-[(4-nitrophenyl)methylene]bis(1H-pyrrole)

: 1430198-57-4
5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

Guidance literature:: (5-{1-[5-(hydroxy-pentafluorophenyl-methyl)-1H-pyrrol-2-yl]-1-methyl-ethyl}-1H-pyrrol-2-yl)-pentafluorophenyl-methanol; 2,2'-[(4-nitrophenyl)methylene]bis(1H-pyrrole); With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.25h;

With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; for 0.583333h;
DOI:10.1021/ja401391z

Reference yield:

: 99840-54-7
5,5'-dimethyldipyrromethane

: 1430198-57-4
5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethylmagnesium bromide / toluene; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 0.5 h / Inert atmosphere

2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 20 °C

3.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

3.2: 0.58 h

With sodium tetrahydroborate; ethylmagnesium bromide; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1021/ja401391z

Reference yield:

: 942041-83-0
5,5-dimethyl-1,9-bis(pentafluorobenzoyly)dipyrromethane

: 1430198-57-4
5,5-dimethyl-10,20-bis(pentafluorophenyl)-15-(4-nitrophenyl)phlorin

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 2 h / 20 °C

2.1: trifluoroacetic acid / dichloromethane / 0.25 h / 20 °C

2.2: 0.58 h

With sodium tetrahydroborate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja401391z