4-phenylthiomethylazulene

Base Information

Chemical Name:4-phenylthiomethylazulene
CAS No.:136006-04-7
Molecular Formula:C₁₇H₁₄S
Molecular Weight:250.364
Hs Code.:

Synonyms:

Suppliers and Price of 4-phenylthiomethylazulene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenylthiomethylazulene

Chemical Property:

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Technology Process of 4-phenylthiomethylazulene

There total 1 articles about 4-phenylthiomethylazulene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17647-77-7
4-methylazulene

: 882-33-7
diphenyldisulfane

: 136006-04-7
4-phenylthiomethylazulene

Guidance literature:: With lithium dicyclohexylamide; Yield given. Multistep reaction; 1.) ether, ice cooling, 40 min, 2.) ice cooling -> RT, 10 min;

Reference yield:

: 136006-04-7
4-phenylthiomethylazulene

: 136006-03-6
2-triphenylmethyldicycloheptaindene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) lithium diisopropylamide / 1.) ether, ice cooling, 10 min, 2.) -78 deg C, 1 h

2: 71 percent / m-chloroperbenzoic acid / CH₂Cl₂ / -78 °C

3: 82 percent / benzene / 3 h / 54 - 65 °C

4: 56 percent / CH₂Cl₂ / -90 -> - 78 deg C, 1 h

5: 21 percent / Ph₃C¹⁺*BF₄^1- / CH₂Cl₂; diethyl ether / 0 deg C -> RT

With trityl tetrafluoroborate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In diethyl ether; dichloromethane; benzene;

Reference yield:

: 136006-04-7
4-phenylthiomethylazulene

: 136006-07-0
C₃₇H₂₈

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) lithium diisopropylamide / 1.) ether, ice cooling, 10 min, 2.) -78 deg C, 1 h

2: 71 percent / m-chloroperbenzoic acid / CH₂Cl₂ / -78 °C

3: 82 percent / benzene / 3 h / 54 - 65 °C

4: 56 percent / CH₂Cl₂ / -90 -> - 78 deg C, 1 h

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane; benzene;