C₁₈H₂₅NO₄

Base Information

Chemical Name:C₁₈H₂₅NO₄
CAS No.:1268249-93-9
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

C<sub>18</sub>H<sub>25</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₂₅NO₄

Chemical Property:

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Technology Process of C₁₈H₂₅NO₄

There total 5 articles about C₁₈H₂₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1268249-92-8
C₂₀H₂₃NO₂

: 1268249-93-9
C₁₈H₂₅NO₄

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; triethylamine; In ethanol; for 18h; under 2327.23 Torr; Inert atmosphere;
DOI:10.1021/ja111540g

Reference yield:

: 93-60-7
methyl 3-pyridinecarboxylate

: 1268249-93-9
C₁₈H₂₅NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: isopropyl alcohol / 18 h / 20 °C / Inert atmosphere

2: Rh(acac)2(CH₂CH₂)2; sodium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl / 1,4-dioxane; water / 60 °C / Inert atmosphere

3: 20 % Pd(OH)2/C; hydrogen / ethanol / 18 h / 2327.23 Torr

4: sodium cyanoborohydride / methanol; acetic acid / 3 h / 20 °C / Inert atmosphere

5: 20 % Pd(OH)2/C; hydrogen; triethylamine / ethanol / 18 h / 2327.23 Torr / Inert atmosphere

With Rh(acac)2(CH₂CH₂)2; 20 % Pd(OH)2/C; hydrogen; sodium cyanoborohydride; sodium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; triethylamine; In 1,4-dioxane; methanol; ethanol; water; acetic acid; isopropyl alcohol;
DOI:10.1021/ja111540g

Reference yield:

: 6516-41-2
1-benzyl-3-(methoxycarbonyl)pyridinium bromide

: 1268249-93-9
C₁₈H₂₅NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: Rh(acac)2(CH₂CH₂)2; sodium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl / 1,4-dioxane; water / 60 °C / Inert atmosphere

2: 20 % Pd(OH)2/C; hydrogen / ethanol / 18 h / 2327.23 Torr

3: sodium cyanoborohydride / methanol; acetic acid / 3 h / 20 °C / Inert atmosphere

4: 20 % Pd(OH)2/C; hydrogen; triethylamine / ethanol / 18 h / 2327.23 Torr / Inert atmosphere

With Rh(acac)2(CH₂CH₂)2; 20 % Pd(OH)2/C; hydrogen; sodium cyanoborohydride; sodium carbonate; (R)-2,2'-bis(diphenylphosphanyl)-1,1'-binaphthyl; triethylamine; In 1,4-dioxane; methanol; ethanol; water; acetic acid;
DOI:10.1021/ja111540g