Technology Process of C17H22BrN3O4S
There total 6 articles about C17H22BrN3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / 0.17 h
1.2: 0.17 h / 0 °C
2.1: N-chloro-succinimide / chloroform
With
N-chloro-succinimide; triethylamine;
In
chloroform;
DOI:10.1016/j.bmcl.2011.06.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium azide; tetrabutylammomium bromide / acetone / 0.5 h
2.1: triphenylphosphine / tetrahydrofuran; water / 5 h
3.1: dichloromethane / 0.02 h
4.1: triethylamine / 0.17 h
4.2: 0.17 h / 0 °C
5.1: N-chloro-succinimide / chloroform
With
N-chloro-succinimide; sodium azide; tetrabutylammomium bromide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; chloroform; water; acetone;
DOI:10.1016/j.bmcl.2011.06.027
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogenchloride / water / 1 h
2.1: sodium azide; tetrabutylammomium bromide / acetone / 0.5 h
3.1: triphenylphosphine / tetrahydrofuran; water / 5 h
4.1: dichloromethane / 0.02 h
5.1: triethylamine / 0.17 h
5.2: 0.17 h / 0 °C
6.1: N-chloro-succinimide / chloroform
With
hydrogenchloride; N-chloro-succinimide; sodium azide; tetrabutylammomium bromide; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; chloroform; water; acetone;
DOI:10.1016/j.bmcl.2011.06.027